Report: Introduction of Laboratory Tools

CHAPTER I
PRELIMINARY
1.1 Background
In conducting
chemical experiments must be used in laboratory equipments such as beaker,
scales, test tube, stative and other. The use of these tools is intended to
support the work of praktikan in experimenting. In conducting chemical
experiments certainly praktikan not apart from substances or chemical solutions
are dangerous, toxic, and flammable.In the lab, it is expected that no errors
in use because it will threaten the safety of praktikan while working. In order
to avoid accidents during practicum, praktikan must have the knowledge and
ability enough to use the tools practicum well, because every tool has
different procedure. Therefore introduction of laboratory equipments like
function and how to use them is needed to facilitate praktikan in Doing practicum,
obtaining accurate data and also for the safety of praktikan.
1.2 Purpose Objectives
1. Students know
the name and function of laboratory equipment
2. Students know
the type, nature and function of chemicals
3. Students know
how to use some laboratory tools
CHAPTER II
LITERATURE REVIEW
The laboratory
is the best place to know the techniques required for consistent and
reproducible analysis (Cairns, 2003).
The laboratory
is a place equipped with equipment for conducting experiments in science or conducting
tests and anlisis.Alat chemical laboratory is an object that digunaka in
activities chemistry laboratories that can be done repeatedly. Examples of
laboratory tools chemistry: test tube, measuring cup, thermometer, spirtus
burner and so forth (Poedjiadi, 1984).
The laboratory
is the best place to know the techniques necessary for consistent and
reproducible analysis (Cairns, 2003)
Laboratory
equipments are the tools we need in the research process or in the lab process.
In practice the introduction of laboratory tools and sterilization tools will
be explained in detail about the function and specification of each tool.
Sterilization is an attempt to free ingredients from undesirable microbes
(Anonymous.2013).
How to use the
tool to avoid misuse and usage. Laboratory tools are also many dangerous tools
such as must be so simple before using the tool we have to sterilize our hand.
If not it can interfere with the process of a study and of course will have an
impact on The results of the study. Attention to the use of laboratory
equipment should be considered for safety and success of work or research. In
the laboratory introduction of laboratory equipment and sterilization tools
will be explained in detail about the function and specification of each tool.
Sterilization is an attempt to free undesirable microbial substances
(Anonymous, 2013).
CHAPTER III
METHODOLOGY
3.1 Tools and materials
1) Cup of
trophies
2) Erlenmeyer
3) Measuring
flask
4) Petridish
5) Measuring cup
6) Glass watch
7) The reaction
tube
8) The vapor
plate
9) Mortal
10) Krush
11) Pipette
drops
12) Pipette
volume
13) Pipette
Mumps
14) Mixer rod
15) Sudip
16) Splitter
17) Desiccator
18) Buret
19) Funnels
20) Shelf tube
raeksi
21) Clamps test
tube
22) Statif and
clamps
23) Brush the
test tube
24) Triangle
25) The suction
ball
26) The spiritus
light
27) Bunsen
28) Three-legs
29) Bottle spray
30) Wire netting
31) Utility
clamps
32) Oven
33) Furnaces
34) Hot plate
35) Analytical
Scales
3.2 How it works
3.2.1 Chemical
Glasses
How to use it is
cleaned, calibrated, then dried with a cloth. Store the solution inside.
3.2.2 Erlenmeyer
Pump
How to use it is
cleaned, calibrated, then dried with a cloth. Then a solution is inserted and
then titrated, then shaken to rotate the erlenmeyer flask.
3.2.3 Measure
Glasses
How to use the
solution is put into a measuring cup. Adjust the required volume. Read the
volume accuracy by looking down the meniscus.
3.2.4 Pipette
How to use it is
cleaned, calibrated, then cleaned with suction paper. Then dip it in solution.
Press the piler then loosen.
3.2.5 Buret
How to use it is
cleaned, calibrated, then dried with a stir bar that is covered with suction
paper. Check the condition of the faucet and the drops are leaking or not. Then
calibrated with the solution to be loaded into the burette, check for bubbles
or not. Open the tap slowly to remove the solution.
3.2.6 Reaction
Tubes
How to use it is
first cleaned then calibrated with aqua DM after that lap with a cloth or wipe
paper. Then the sample to be reacted is inserted into the test tube.
3.2.7 Glass
Watch
How to use it is
first cleaned with a tissue or a cloth, then put on top of a beaker if used as
a glass beaker, or place the chemical to be weighed on the glass.
3.2.8 Funnels
Place the funnel
over Erlenmeyer's mouth or burette, slowly insert the field into the mouth of
the funnel.
3.2.9 Grail
Insert the
ingredients or solution to be vaporized over the cup. After that heat or steam
into the oven.
3.2.10 Mortar
and Pastle
How to use it is
to enter the chemical in the form of solids into mortar (mortar) and gerus
until smooth using alu (pastle).
3.2.11 Spatula
Take a material
or a substance in the form of solids with a spatula, then place it in a place
to store materials such as a watch glass.
3.2.12 Mixer rod
Stir the
solution in the beaker with a stirring stick, then observe.
3.2.13 Wire
Netting
Place the wire
netting on top of Bunsen with three legs. Then put a glass tool in which the
solution will be heated.
3.2.14 Leg Three
How to use it is
placed between Bunsen and wire netting.
3.2.15 Pumpkin
Measure
How to use it is
cleaned, calibrated, then cleaned with a washcloth. Then put the solution to
dilute or insert the substance with the help of suction paper, so that the
substance does not stick to the wall above the upper limit. Then put the
aquadest to dissolve it. Then fit it with the lower border. Close then
homogenize.
3.2.16
Thermometer
How to use the
thermometer is inserted into a solution and then consider the temperature of
the solution or the temperature changes that occur.
3.2.17 Reaction
Tube Rack
How to use it is
to place the test tube into the holes that exist in the rack of the test tube.
CHAPTER IV
OBSERVATION RESULT
4.1 Results of observation
No
|
Name
|
Function
|
1
|
beaker
|
-Where to store the solution
-Place to heat the chemical solution, to evaporate
solvent / solvent or to concentrate
|
2
|
Erlenmeyer
|
-Place reacting substances and / or mixing
substances
-Used as a place of substance to be titrated
|
3
|
Volumetric
flask
|
-Place the
solution and dilute the solution
|
4
|
Petri Dish
|
- A place for microbial breeding
|
5
|
Measuring cup
|
-To measure the volume of the solution
|
6
|
Watch glass
|
-As a container for weighing
|
7
|
Test tube
|
-To react two or more substances on a small scale
|
8
|
Vaporizer cup
|
-To dry a material in a desiccant oven
|
9
|
Mortar and pestle
|
-To soften substances that are still solid or
crystalline
|
10
|
Krush
|
-Made of porcelain, inert.
-Used to heat metal metals, for example ash content
of metals and other materials
|
11
|
Drop pipette
|
-To drip or take the solution in small amounts
|
12
|
Pipette volume
|
-To measure the volume of the solution
|
13
|
Pipette Mumps
|
-To take the solution at a certain volume
|
14
|
Stirring bar
|
-To stir or shake an ingested substance
|
15
|
Sudip
|
-To take chemicals in solid form, for example in the
form of crystals
|
16
|
Split funnel
|
-To separate two non-mixed solutions due to
differences in density, usually used in the extraction process
|
17
|
Desiccator
|
-To store materials that must be free of water and
to dry substances in the laboratory, there are two types of desensors namely
the usual desiccator and vacuum desiccator
|
18
|
Buret
|
-Used for titration and at a certain level can also
be used to measure the volume of a solution
|
19
|
Funnel
|
-To insert or remove the solution from one place to
another and also used for filtration process after having the filter paper on
top
|
20
|
Tube shelf reaction
|
- To place the test tube
|
21
|
Clamp the test tube
|
- Clamping the test tube
|
22
|
Stative and clamps
|
-Clamping the socket on the extraction process
-Clamping the burette on the titration process
-Clamping the condenser to the distillation process
|
23
|
Brush the test tube
|
-To brush the test tube while washing it
|
24
|
Triangle
|
- To place the cup / erlenmeyer when heated
|
25
|
The suction ball
|
-To suck out the solution to be removed from the
solution bottle
|
26
|
Spark light
|
- To burn the substance / heating solution
|
27
|
Bunsen
|
-To heat the solution, and can also be used for
sterilization in a process
|
28
|
Tripod
|
-To buffer the spirtus burner
|
29
|
Spray bottle
|
-Place put aquades
|
30
|
Wire netting
|
-To hold pumpkin or beaker during heating time, use
spritus heater or bunsen heater
|
31
|
Utility clamps
|
-To clamp a glass tool such as, erlenmeyer, cup,
etc.
|
32
|
Oven
|
-To dry tools before use, and to dry materials that
are wet
|
33
|
furnace
|
- Determining ash content
|
34
|
Hot plate
|
-As a heater
|
35
|
Analytical Scales
|
-To weigh substances
|
CHAPTER V
DISCUSSION
4.1 Discussion
1. Glasses of chemicals
The large, large-diameter tall glass,
made of heat-resistant borosilicate glass, serves to measure the volume of a
solution that does not require high levels of precision, holds chemicals, heats
liquids and heating liquids. How to use it is cleaned, calibrated, then dried
with a cloth. Store the solution inside.
2. Erlenmeyer
In the form of a glass whose diameter is
increasingly upwards by the scale along its wall, it serves to store and heat
the way it is cleaned, calibrated, and dried with a cloth. Then a solution is
inserted and then titrated, then shaken to rotate the erlenmeyer flask,
accommodate filtrate of filtrate, and hold the titrant (the titrated solution)
in the filtration process.
3. Pump size
Pumpkin with a long, closed neck, made
of glass and should not be exposed to heat because it can expand to function to
make a solution with a certain concentration and dilute the solution. How to
use it is cleaned, calibrated, then cleaned with a washcloth. Then put the
solution to dilute or insert the substance with the help of suction paper, so
that the substance does not stick to the wall above the upper limit. Then put
the aquadest to dissolve it. Then fit it with the lower border. Close then
homogenize.
4.Petridish
A place to breed microbes.
5. Measuring cup
In the form of tall glass with a scale
along the wall, made of glass or plastic that is not heat resistant, serves to
measure the volume of the solution does not require a high level of accuracy in
a certain amount.
6. Glass watch
Made of clear glass and has various
sizes serving as a glass beaker when heating samples, a place when weighing
chemicals, and a place to dry solids in a desiccator. How to use it is first
cleaned with a tissue or a cloth, then put on top of a beaker if used as a
glass beaker, or place the chemical to be weighed on the glass.
7. Test tube
The tubes are sometimes equipped with a
lid, made of heat-resistant borosilicate glass, serves as a place to react
chemicals and to perform chemical reactions on a small scale. How to use it is
first cleaned then calibrated with aqua dm after that lap with a cloth or paper
suction. Then the sample to be reacted is inserted into the test tube.
8. Cup
Made of porcelain, serves to expose the
solution. Put the ingredients or solution to be vaporized over the cup. After
that heat or steam into the oven
9. Mortar and Pastle
Made of glass, porcelain, or granite
stone serves to destroy and mix solids. How to use it is to enter the chemical
in the form of solids into the mortar (Mortar) and gerus until smooth using
pestle (Pastle).
10.Krush
Made of persolene and is inert,
used to heat metals.
11.Pipet drops
To drip or take a solution with a small
amount
12. Pipette volume
To measure the volume of the solution
13. Pipette Mumps
The means to extract a certain amount of
liquid or free quantity, to take a certain amount of fluid appropriately
(pipette of size), to measure and remove a solution with a certain volume
(pipette of size), and to take a liquid on a small scale (pipette drops) . How
to use the solution is put into a measuring cup. Adjust the required volume.
Read the volume accuracy by looking down the meniscus.
14. Stirring rod
Made of heat-resistant glass serves to
stir chemical liquids in a beaker. Stir the solution in the beaker with a
stirring stick, then observe.
15. Sudip / Spatula
Form of a long spoon with flat top tip,
made of stainless steel or aluminum serves to take the chemical in the form of
solids and used to stir the solution. Take a material or a substance in the
form of solids with a spatula, then place it in a place to store materials such
as a watch glass.
16. Splitter
Made of plastic or heat-resistant glass
and has a stemware-like shape, consisting of a long, short-stem mouthpiece to
separate two non-mixed solutions due to the difference in density. Separate
funnel is used in the extraction process.
17.desikator
To store materials that must be
water-free and dry the substances in the laboratory. Known two types of
desiccers namely the usual desiccator and vacuum desiccator.
18 Buret
Form a striped glass tube and has a
valve diujungnya, serves to remove a solution with a certain volume, usually
used for titration. How to use it is cleaned, calibrated, then dried with a
stir bar that is covered with suction paper. Check the condition of the faucet
and the drops are leaking or not. Then calibrated with the solution to be
loaded into the burette, check for bubbles or not. Open the tap slowly to
remove the solution.
19. Funnel
Used to insert or inject a filtering
solution after filtered paper.
20 Reaction tube shelf
The reaction tube rack is made of wood
with holes the size of the test tube serves as a place to put the test tube.
How to use it is to place the test tube into the holes that exist in the rack
of the test tube.
21.Pack the test tube
To clamp the test tube.
22.Stative and clamps
As a brace, for example:
- To clamp the socket on the extraction
process
- Clamping the burette in the titration
process
- To clamp the condenser in the
distillation process
23 Brush the test tube
To clean the test tube after use for the
lab.
24. Triangle
To hold the container, for example a
crucible during heating or a funnel at the time of filtration.
25.B suction ball
To suck out the solution to be removed
from the solution bottle
26.Lights spritus
To heat the solution and can also be
used for sterilization in the process of a process.
27.Bunsen
To heat the solution, and can also be
used for sterilization in a process
28. Legs three
The iron buffer ring serves to hold the
wire netting in the heating. How to use it is placed between bunsen and wire
netting.
29. Bottle spray
Place put aquades.
30. Wire screen
Wire coated with asbestos serves as a
base in the heat dissemination from a barrier. Place the wire netting on top of
the bunsen with three foot supports. Then put a glass tool in which the
solution will be heated
31.Klem utilities
To clamp a glass tool such as,
erlenmeyer, cup, etc.
32.Oven
To dry the tools before use and is used
to dry the material in wet condition.
33.Tanur
Used as a heater at high temperatures,
about 1000 ° c.
34.Hot plate
To heat the solution. Usually for
flammable solutions.
35. Analytical Scales
To weigh substances
CHAPTER VI
COVER
6.1 Conclusions
1. After practicing practicum can know
the names and functions of laboratory equipment.
2. Each type of chemical substance has
different properties, such as acid that is corrosive to the surrounding
objects, in addition chemicals have the same function.
3. After practicing practicum can know
how to use some laboratory tools, Laboratory tools have different functions and
ways of using.
6.2 Suggestions
Preferably at the time of practicum we
all must maintain the condition of the condition of the room for the lab work
safely and smoothly.
CHAPTER VII
BIBLIOGRAPHY
Anonymous. 2013. Tools Pratikum Kimia.
Www.scribd.com. Accessed October 25, 2013
Braddy, James E. 1994. Chemistry
University Edition Fifth. Jakarta: Erlangga.
Cairns, Donald. 2003. Intisari Kimia Farmasi Edisi Kedua.
Buku Kedokteran EGC. Jakarta.
Http://apriansyaabdullah.blogspot.co.id/2014/03/example-report-praktikum-
introduction.html
How to drip solution using dropper drops correctly?
BalasHapusThe pipette is loaded slowly up to 2 cm from the propacket.
HapusClick on the propetet to deflect
Enter the tip of the pipette into the liquid and then release the tip of the pipette slowly then the liquid akn rise to the top of the pipette slowly
Then push the propipet again slowly to remove the liquid from the teste dalan.
If the liquid in use is not dangerous then the flow can be arranged by hand.
Give me a description about report? And the correct structure of report..
BalasHapuslab report format:
Hapusname
date lab was finished
title of lab
IB chemistry SL/HL
Introduction:
-Explanation of topic
-chemical explanations
-reactions
-normal stuff
-purpose
-variables
-hypothesis
-controls
materials:
1. chemical, formula, volume
2. type of flask, size, amount needed
3. etc.
method:
paragraf format
-first, then, next, finally, etc.
row data:
-just data collected
-data tables (tittle and explanation)
why you use Hot plate in your experiment?
BalasHapusTo prove the usefulness of hot plate, ie heating solution. Usually for flammable solutions.
Hapus"Dried with a cloth" what would happen if the tool was not drained. Please explain?
BalasHapusIf the apparatus is not drained before use, the residual water after washing attached to the appliance will be mixed in the solution or substance used in the experiment. It will affect the reaction that occurs and of course the results of experiments obtained did not match the expected.
HapusWhat First aid should be given when the hand is exposed to harmful chemicals ?
BalasHapusWhen exposed to acid on the skin immediately wash with enough water then neutralize with 5% ammonia solution. Whereas if exposed to base on the skin immediately wash with enough water and neutralize with a solution of 4% boric acid or 1% acetic acid.
HapusDoes the laboratory need to wear labor safety goggles?
BalasHapusYes necessary, because safety glasses will protect the eyes from sparks of chemicals.
HapusI've been described by a lecturer's assistant that a good bunsen is a bunsen that produces a blue flame why is that so?
BalasHapusBunsen burners can generally be used to produce three types of fire. A yellow or orange fire is usually the coolest and is also known as fire safety. This usually flames tests before setting the stove for other types of applications. It just shows that the stove is on. The temperature of the fire safety forecast is 300 degrees Celsius
HapusMedium flame blue flame or visible flame .. This is called visible fire because it is very difficult to know in brightly lit room. The medium fire temperature is about 500 degrees centigrade. This is one of the most common fires used in Bunsen burners
The hottest flame that can be produced by this Bunsen burner. Called a roaring blue fire. The temperature of this flame is 700 degrees Celsius or more. The main feature of this flame is the right blue triangle of light in the middle. It is also the only fire that makes a sound while burning.
A blue flame which is often said to be a good bunsen flame as it is considered best suited to the burning or heating needs of the laboratory substances.
What are the effects that occur if the lab is not appropriate procedure
BalasHapusTry to explain the usual vacuum desiccator?
BalasHapusCommon desiccators are made of semi-boroxylate, plastic or mica type glasses. Type glass or amber. Inside the desiccator there is a porous disc made out of porcelain used to lay the glassware. Below the porcelain dish there is a drying material generally made of; Silicates, concentrated sulfuric acid, phofor pentaoxide, calcium oxide and so on. Silicone dryers are usually given a blue indicator of the keriing and if it has binding water vapor color will turn red. Silicagels that have been saturated with water vapor can be dried again by heating in an oven with a temperature of 100 °. The desiccator cover on the surface should be given pelican material eg: silicon grease, to be covered more tightly.
Hapus